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By Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Ralf RIEDEL Technical University of Darmstadt, Germany Alexander G. MERZHANOV ISMAN, Russia Chang-Chun

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Yin, T. Sato, and F. , 87 (2004) 1161 [11] D. Huang, S. Liao, J. Liu, Z. Dang, J. Photochem. Photobiol. , 184 (2006) 282 [12] J. Xu, J. Lia, W. Dai, Y. Cao, H. Li, K. Fan, Appl. Catal. , 79 (2008) 72 [13] J. He, J. Zhao, T. Shen, H. Hidaka, N. Serpone, J. Phys. Chem. B, 101 (1997) 9027. [14] J. Yu, J. Xiong, B. Cheng, Y. Yu, J. Wang, J. , 178 (2005) 1968. H. Y. Li, J. Phys. Chem. , 112 (2008) 5405. C. G. K. T. Z. Zhang, Chem. , 14 (2002) 3808. [17] W. Choi, A. R. Hoffmann, J. Phys. , 98 (1994) 13669.

AlN is visible from 1500°C. The same phenomenon is observed on samples treated in the big furnace. Nitridation is expected to be complete at 1200°C, according to Fig. 1. Fig. b shows traces of AlN at 1300°C. This is due to the treatment duration. A longer treatment is expected to lead to a higher nitridation rate. This is confirmed by Fig. 5 that shows XRD patterns of samples treated at 1400°C for 8 hours in the small furnace and at 1200°C for 8 hours in the big furnace. Fig. 6 and 7 show EDX maps and backscattered electrons micrographs of the as-treated samples.

J. S. B. Kim: J. Mater. Sci. Lett. Vol. 17 (1998), p. 24 Synthesis of alumina and aluminum nitride layers on a graphitic substrate via a sol-gel route. fr Keywords: Sol-gel process, aluminum nitride, carbothermal nitridation, thermodynamics. Abstract In this study, our objective is to deposit an alumina or an aluminum nitride layer on a turbostratic carbon substrate. The coatings are synthesized via a sol-gel route followed by a heat treatment in order to obtain α-alumina or hexagonal aluminum nitride by carbothermal nitridation of alumina.

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12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART B including: Symposium by Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Ralf RIEDEL Technical University of Darmstadt, Germany Alexander G. MERZHANOV ISMAN, Russia Chang-Chun


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